Senior Research Associate (X-Ray Crystallography)
Chemical Crystallography
Crystallographic methods provide detailed atomic-level descriptions of crystalline solids, including molecular structure and geometrical information on intermolecular interactions.
Single-crystal and powder X-ray diffraction are core analytical techniques within the chemical sciences, which support and augment a broad range of research within the Department. Modern diffraction instruments, applied at both laboratory and synchrotron sources, enable complex chemical problems to be tackled using crystallographic methods: for example, characterizing and understanding the consequences of disorder in molecular crystals or monitoring chemical changes in single crystals or crystalline powders.
Publications
Synchrotron X-ray study of [5,15-diphenyl-2,8,12,18-tetra-n-hexyl-3,7,13,17-tetramethylporphyrinato]nickel(II)
– Acta Crystallographica Section E: Crystallographic Communications
(2003)
59,
M818
(doi: 10.1107/s1600536803018853)
3-(trimethylsilylethynyl)carbazole
– Acta Crystallographica Section E: Crystallographic Communications
(2003)
59,
O1342
(doi: 10.1107/s1600536803017963)
Applications of manganocene in the synthesis of Mn(II) amide and imide cages
– Dalton Transactions
(2003)
3002
(doi: 10.1039/b303727b)
Synthesis, structure and magnetic characterisation of a new layered ammonium manganese(ii) diphosphate hydrate , (NH 4 ) 2 [Mn 3 (P 2 O 7 ) 2 (H 2 O) 2 ]
– Journal of Materials Chemistry
(2003)
13,
1950
(doi: 10.1039/b304003h)
The synthesis and characterisation of the cluster dianion [PtRu5C(CO)15]2- and its reactions with Au and Pt cationic fragments produced in situ
– Dalton Transactions
(2003)
2651
(doi: 10.1039/b303178k)
Hydronium pentaaquacopper(II) triperchlorate
– Acta Crystallographica Section E: Crystallographic Communications
(2003)
59,
i105
(doi: 10.1107/s1600536803014272)
The synthesis and characterisation of the cluster dianion [ptRu5C(CO)15]2- and its reactions with Au and Pt cationic fragments produced in situ
– Journal of the Chemical Society. Dalton Transactions
(2003)
3,
2651
(doi: 10.1039/b303178k)
Complexation of Diphenyl(phenylacetenyl)phosphine to Rhodium(III) Tetraphenyl Porphyrins: Synthesis and Structural, Spectroscopic, and Thermodynamic Studies
– Inorganic Chemistry
(2003)
42,
3086
(doi: 10.1021/ic026257a)
Improved Synthesis of Dithieno[3,2‐b:2′,3′‐d]thiophene (DTT) and Derivatives for Cross Coupling.
– ChemInform
(2003)
34,
no
(doi: 10.1002/chin.200310110)
Supramolecular architectures of cyclohexane-1, 3cis, 5cis-tricarboxylic acid in acid : base complexes
– New Journal of Chemistry
(2003)
27,
365
(doi: 10.1039/b208686g)
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