A UNIQUE LITHIUM HALIDE COMPLEX, [(LIBR)2.3HMPA.TOLUENE] - SYNTHESIS FROM REACTION OF SOLID NH4BR WITH BUNLI IN HMPA (HEXAMETHYLPHOSPHORAMIDE) TOLUENE MEDIA, CRYSTAL-STRUCTURE SHOWING 2 LI-BR UNITS LINKED BY 3 MU-2-HMPA LIGANDS, AND DETECTION OF LI-7 ... P-31 COUPLING IN SOLUTIONS OF THE COMPLEXH
D BARR, MJ DOYLE, RE MULVEY, PR RAITHBY, D REED, R SNAITH, DS WRIGHT
– Chemical Communications
(1989)
318
(DOI: 10.1039/c39890000318)
Reaction of solid sodium hydride with solid ammonium thiocyanate in HMPA-toluene: An ESR spectroscopic investigation and crystal structures of the two products of the reaction, [(NaNCS·HMPA)2]∞ and (NaNCS·2HMPA)2
D BARR, MJ DOYLE, SR DRAKE, PR RAITHBY, R SNAITH, DS WRIGHT
– Polyhedron
(1989)
8,
215
SYNTHESIS, AND CRYSTAL AND SOLUTION STRUCTURES OF THE 1-1 TMEDA COMPLEX OF LITHIUM THIOCYANATE, (LISCN.TMEDA)N [TMEDA = ME2N(CH2)2NME2] - A POLYMERIC SOLID WITH LI+ IONS LINKED BY BIFUNCTIONAL LINEAR SCN- LIGANDS
D BARR, MJ DOYLE, RE MULVEY, PR RAITHBY, R SNAITH, DS WRIGHT
– J. Chem. Soc., Chem. Commun.
(1988)
145
(DOI: 10.1039/c39880000145)
Evidence for a radical-forming process during the reaction of solid NH<sub>4</sub>SCN with n-butyl-lithium and hexamethylphosphosphoramide (HMPA) in toluene: crystal structure of the product, (LiNCS·2HMPA)<sub>2</sub>
D BARR, MJ DOYLE, SR DRAKE, PR RAITHBY, R SNAITH, DS WRIGHT
– Chemical Communications
(1988)
1415
(DOI: 10.1039/c39880001415)
A Li<sub>8</sub>cluster of three edge-connected Li<sub>4</sub>tetrahedra held by Li–N, Li ⋯ C, and Li ⋯ Li interactions: crystal structure of (o-LiC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>·NLi·CH<sub>2</sub>CH<sub>2</sub>NMe<sub>2</sub>)<sub>4</sub>and detection of metal ⋯ metal coupling within it by<sup>7</sup>Li COSY n.m.r. spectroscopy
D BARR, W CLEGG, SM HODGSON, RE MULVEY, D REED, R SNAITH, DS WRIGHT
– Chemical Communications
(1988)
367
(DOI: 10.1039/c39880000367)
Isolation and solution structures of {PhCH2NLiCH2CH2NMe2}n and of the totally rigid dilithium compound, {o-LiC6H4CH2NLiCH2CH2NMe2}n; evidence for Li…o-HC interactions
D BARR, R SNAITH, DS WRIGHT, RE MULVEY, K JEFFREY, D REED
– Journal of Organometallic Chemistry
(1987)
325,
c1
(DOI: 10.1016/0022-328x(87)80411-4)
Three model structural types in lithium amide chemistry: the crystal and molecular structures of dimeric [Ph(Me)NLi·TMEDA]<sub>2</sub>(TMEDA = Me<sub>2</sub>NCH<sub>2</sub>CH<sub>2</sub>NMe<sub>2</sub>) and monomeric Ph(naphthyl)NLi·PMDETA [PMDETA = MeN(CH<sub>2</sub>CH<sub>2</sub>NMe<sub>2</sub>)<sub>2</sub>], and of [Ph(naphthyl)NLi·TMEDA]<sub>2</sub>, a ‘loose dimer’
D BARR, W CLEGG, RE MULVEY, R SNAITH, DS WRIGHT
– Chemical Communications
(1987)
716
(DOI: 10.1039/c39870000716)