Intramolecular versus intermolecular bonding in amidoantimony dimers; syntheses and structures of {Sb(NMe 2 )[µ-N(mpy)]} 2 (mpy = 4-methylpyridin-2-yl) and [Sb(NMe 2 ){µ-N[C 6 H 2 (OMe) 3 -3,4,5]}] 2
AJ EDWARDS, MA PAVER, MA RENNIE, PR RAITHBY, CA RUSSELL, DS WRIGHT
– J. Chem. Soc., Dalton Trans.
(1994)
2963
(DOI: 10.1039/dt9940002963)
Dimeric antimony complexes capturing dimethylamine as a neutral donor; syntheses and structural characterisation of [SbCl<sub>2</sub>(NHMe<sub>2</sub>)(µ-OEt)]<sub>2</sub>and [SbCl(NHMe<sub>2</sub>)(µ-NBu<sup>t</sup>)]<sub>2</sub>
AJ EDWARDS, NE LEADBEATER, MA PAVER, PR RAITHBY, CA RUSSELL, DS WRIGHT
– J. Chem. Soc., Dalton Trans.
(1994)
1479
(DOI: 10.1039/dt9940001479)
Structure of bis(pentamethyldiethylenetriamine)disodium hexasulfide
S BESSER, R HERBSTIRMER, D STALKE, AT BROOKER, R SNAITH, DS WRIGHT
– Acta Crystallographica Section C: Structural Chemistry
(1993)
49,
1482
(DOI: 10.1107/s0108270193001167)
A thiouracil-Ca2+ complex containing two tautomeric forms of the thiouracilyl anion: Synthesis and crystal structure of [(thiouracilyl)2Ca·2DMSO·H2O]2
FA BANBURY, MG DAVIDSON, AJ EDWARDS, MIL SOLERA, PR RAITHBY, R SNAITH, D STALKE, DS WRIGHT
– Inorganica Chimica Acta
(1993)
203,
93
Dalton communications. The ‘broken cube’ polymer structure of (LiBr·thf) ∞ (thf = tetrahydrofuran)
AJ EDWARDS, MA PAVER, PR RAITHBY, CA RUSSELL, DS WRIGHT
– J. Chem. Soc., Dalton Trans.
(1993)
3265
(DOI: 10.1039/dt9930003265)
A model intermediate for the nucleophilic substitution of (Cp) 2 Sn; synthesis and structure of (Cp)(Me 3 Si) 2 NSn(µ-Cp)Li·pmdeta [Cp = C 5 H 5 , pmdeta =(Me 2 NCH 2 CH 2 ) 2 NMe]
MA PAVER, CA RUSSELL, D STALKE, DS WRIGHT
– J. Chem. Soc., Chem. Commun.
(1993)
1349
(DOI: 10.1039/c39930001349)
THE 1ST IMINO-LEAD COMPLEX - SYNTHESIS AND X-RAY CHARACTERIZATION OF PB[MU-N=C(BU(T))PH](3)LITHF (THF = TETRAHYDROFURAN)
AJ EDWARDS, MA PAVER, PR RAITHBY, CA RUSSELL, DS WRIGHT
– J. Chem. Soc., Chem. Commun.
(1993)
1086
(DOI: 10.1039/c39930001086)
Two triorganostannate complexes synthesised from bis(cyclopentadienyl)tin(<scp>II</scp>); structural variation between [Mg(thf)<sub>6</sub>]<sup>2+</sup>2[Sn(η<sup>3</sup>-C<sub>5</sub>H<sub>5</sub>)<sub>3</sub>]<sup>–</sup>and [Li(thf)<sub>4</sub>]<sup>+</sup>[Sn(C<sub>13</sub>H<sub>9</sub>)<sub>3</sub>]<sup>–</sup>(thf = tetrahydrofuran, C<sub>13</sub>H<sub>9</sub>= fluorenyl)
AJ EDWARDS, MA PAVER, PR RAITHBY, CA RUSSELL, D STALKE, A STEINER, DS WRIGHT
– Dalton Transactions
(1993)
1465
(DOI: 10.1039/dt9930001465)
Synthesis and crystal structure of Sb(NCPh<sub>2</sub>)<sub>3</sub>
AJ EDWARDS, MA PAVER, PR RAITHBY, CA RUSSELL, DS WRIGHT
– Dalton Transactions
(1993)
2257
(DOI: 10.1039/dt9930002257)
Metal-mediated conversion of a 5-aminothiatriazole into a 5-mercaptotetrazolyl ligand by reaction with a solid metal hydroxide: synthesis and crystal structure of [naphthylN·N[double bond, length half m-dash]N·N[horiz bar, double dot above]C([horiz bar, double dot above]S)] 2 Ba·3HMPA
FA BANBURY, MG DAVIDSON, A MARTIN, PR RAITHBY, R SNAITH, KL VERHOREVOORT, DS WRIGHT
– Chemical Communications
(1992)
1152
(DOI: 10.1039/c39920001152)
The first calcium–mercury cocomplex: synthesis and crystal structure
MG DAVIDSON, SC LLEWELLYN, MIL SOLERA, PR RAITHBY, R SNAITH, DS WRIGHT
– Chemical Communications
(1992)
573
(DOI: 10.1039/c39920000573)
Isolation, structure and MO calculational investigations of a highly stable, hydrogen-bonded primary amine–phosphine oxide adduct, 2-aminobenzothiazole–HMPA, C<sub>6</sub>H<sub>4</sub>SC(N)NH<sub>2</sub>OP(NMe<sub>2</sub>)<sub>3</sub>; a possible model to explain the carcinogenicity of HMPA (HMPA = hexamethylphosphoramide)
DR ARMSTRONG, S BENNETT, MG DAVIDSON, R SNAITH, D STALKE, DS WRIGHT
– J. Chem. Soc., Chem. Commun.
(1992)
262
(DOI: 10.1039/c39920000262)
The observation of a Pb–Li bond; synthesis, structure and model molecular orbital (MO) calculations on the monomeric Ph<sub>3</sub>Pb–Li·(pmdeta) complex [pmdeta =(Me<sub>2</sub>NCH<sub>2</sub>CH<sub>2</sub>)<sub>2</sub>NMe]
DR ARMSTRONG, MG DAVIDSON, D MONCRIEFF, D STALKE, DS WRIGHT
– J. Chem. Soc., Chem. Commun.
(1992)
1413
(DOI: 10.1039/c39920001413)
The stabilisation of water as a ligand in lithiated organic compounds: intra- and inter-molecular hydrogen bonding in the structures of the aquo complexes [Li·HMPA·H2O]2 and [Li·HMPA]2·H2O
DR ARMSTRONG, D BARR, PR RAITHBY, R SNAITH, DS WRIGHT, PV SCHLEYER
– Inorganica Chimica Acta
(1991)
185,
163
Lithiations of mercaptoamines containing NC(S)NH–,–NHC(S)S– and –NHC(S)NH– units: syntheses, crystal structures and model molecular-orbital calculations
DR ARMSTRONG, RE MULVEY, D BARR, RW PORTER, PR RAITHBY, TRE SIMPSON, R SNAITH, DS WRIGHT, K GREGORY, P MIKULCIK
– Dalton Transactions
(1991)
765
(DOI: 10.1039/dt9910000765)
Unusual routes to complexes of binary alkali metal–non-metal compounds: preparations and crystal and solution structures of Li<sub>2</sub>S<sub>6</sub>·(tmeda)<sub>2</sub>(tmeda = etramethylethylenediamine), and synthetic extensions of the routes
AJ BANISTER, D BARR, AT BROOKER, W CLEGG, MJ CUNNINGTON, MJ DOYLE, SR DRAKE, WR GILL, K MANNING, PR RAITHBY, R SNAITH, K WADE, DS WRIGHT
– J. Chem. Soc., Chem. Commun.
(1990)
105
(DOI: 10.1039/c39900000105)
The first lithiated organic compound containing water as a ligand: synthesis and crystal structure of 2-mercaptobenzoxazolyl(tetramethylethylenediamine)lithium monohydrate, C<sub>6</sub>H<sub>4</sub>OC(S)NLi(tmeda)H<sub>2</sub>O, a model acid–base intermediate
D BARR, PR RAITHBY, PV SCHLEYER, R SNAITH, DS WRIGHT
– Chemical Communications
(1990)
643
(DOI: 10.1039/c39900000643)
[H2C(CH2)5NLI]6, THE 1ST CYCLIZED LITHIUM AMIDE LADDER - SYNTHESIS AND STRUCTURE OF HEXAMETHYLENEIMIDOLITHIUM
D BARR, W CLEGG, SM HODGSON, GR LAMMING, RE MULVEY, AJ SCOTT, R SNAITH, DS WRIGHT
– ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH
(1989)
28,
1241
Dilithiation of N,N′-diphenylthiourea, PhNHC(S)NHPh, in HMPA: the unexpected structure of the product, [PhNPh)SLi·2HMPA]2, and supporting ab initio MO calculations on model systems
DR ARMSTRONG, RE MULVEY, D BARR, R SNAITH, DS WRIGHT, W CLEGG, SM HODGSON
– Journal of Organometallic Chemistry
(1989)
362,
C1
(DOI: 10.1016/0022-328x(89)85298-2)
Reaction of solid sodium hydride with solid ammonium thiocyanate in HMPA-toluene: An ESR spectroscopic investigation and crystal structures of the two products of the reaction, [(NaNCS·HMPA)2]∞ and (NaNCS·2HMPA)2
D BARR, MJ DOYLE, SR DRAKE, PR RAITHBY, R SNAITH, DS WRIGHT
– Polyhedron
(1989)
8,
215