Two triorganostannate complexes synthesised from bis(cyclopentadienyl)tin(II); structural variation between [Mg(thf)6]2+2[Sn(η3-C5H5)3]–and [Li(thf)4]+[Sn(C13H9)3]–(thf = tetrahydrofuran, C13H9= fluorenyl)
J. Chem. Soc., Dalton Trans.
(1993)
1465
(doi: 10.1039/dt9930001465)
Synthesis and crystal structure of Sb(N[double bond, length half m-dash]CPh 2 ) 3
J. Chem. Soc., Dalton Trans.
(1993)
2257
(doi: 10.1039/dt9930002257)
Dalton communications. The ‘broken cube’ polymer structure of (LiBr·thf)∞(thf = tetrahydrofuran)
J. Chem. Soc., Dalton Trans.
(1993)
3265
(doi: 10.1039/dt9930003265)
Isolation, structure and MO calculational investigations of a highly stable, hydrogen-bonded primary amine–phosphine oxide adduct, 2-aminobenzothiazole–HMPA, C6H4SC(N)NH2OP(NMe2)3; a possible model to explain the carcinogenicity of HMPA (HMPA = hexamethylphosphoramide)
J. Chem. Soc., Chem. Commun.
(1992)
262
(doi: 10.1039/c39920000262)
The observation of a Pb–Li bond; synthesis, structure and model molecular orbital (MO) calculations on the monomeric Ph 3 Pb–Li·(pmdeta) complex [pmdeta =(Me 2 NCH 2 CH 2 ) 2 NMe]
J. Chem. Soc., Chem. Commun.
(1992)
1413
(doi: 10.1039/c39920001413)
Metal-mediated conversion of a 5-aminothiatriazole into a 5-mercaptotetrazolyl ligand by reaction with a solid metal hydroxide: synthesis and crystal structure of [naphthylN·NN·NC(S)]2Ba·3HMPA
Chemical Communications
(1992)
1152
(doi: 10.1039/c39920001152)
The first calcium–mercury cocomplex: synthesis and crystal structure
Chemical Communications
(1992)
573
(doi: 10.1039/c39920000573)
The stabilisation of water as a ligand in lithiated organic compounds: intra- and inter-molecular hydrogen bonding in the structures of the aquo complexes [Li·HMPA·H2O]2 and [Li·HMPA]2·H2O
Inorganica Chimica Acta
(1991)
185
163
Lithiations of mercaptoamines containing NC(S)NH–,–NHC(S)S– and –NHC(S)NH– units: syntheses, crystal structures and model molecular-orbital calculations
Dalton Transactions
(1991)
765
(doi: 10.1039/dt9910000765)
Unusual routes to complexes of binary alkali metal–non-metal compounds: preparations and crystal and solution structures of Li2S6·(tmeda)2(tmeda = etramethylethylenediamine), and synthetic extensions of the routes
Chemical Communications
(1990)
105
(doi: 10.1039/c39900000105)
The first lithiated organic compound containing water as a ligand: synthesis and crystal structure of 2-mercaptobenzoxazolyl(tetramethylethylenediamine)lithium monohydrate, C6H4OC(S)NLi(tmeda)H2O, a model acid–base intermediate
J. Chem. Soc., Chem. Commun.
(1990)
643
(doi: 10.1039/c39900000643)
[H2C(CH2)5NLI]6, THE 1ST CYCLIZED LITHIUM AMIDE LADDER - SYNTHESIS AND STRUCTURE OF HEXAMETHYLENEIMIDOLITHIUM
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH
(1989)
28
1241
Dilithiation of N,N′-diphenylthiourea, PhNHC(S)NHPh, in HMPA: the unexpected structure of the product, [PhNPh)SLi·2HMPA]2, and supporting ab initio MO calculations on model systems
Journal of Organometallic Chemistry
(1989)
362
C1
(doi: 10.1016/0022-328X(89)85298-2)
2 MONOMERIC, OCTAHEDRAL COMPLEXES OF ALKALINE-EARTH METAL-SALTS - SYNTHESES, PHYSICAL CHARACTERISTICS, AND CRYSTAL-STRUCTURES OF SRI2.4HMPA AND SR(NCS)2.4HMPA [HMPA=O-P(NME2)3]
Chemical Communications
(1989)
893
(doi: 10.1039/c39890000893)
REACTION OF SOLID SODIUM HYDRIDE WITH SOLID AMMONIUM THIOCYANATE IN HMPA-TOLUENE - AN ESR SPECTROSCOPIC INVESTIGATION AND CRYSTAL-STRUCTURES OF THE 2 PRODUCTS OF THE REACTION, [(NANCS.HMPA)2] INFINITY AND (NANCS.2HMPA)2
Polyhedron
(1989)
8
215
A unique lithium halide complex, [(LiBr) 2 ·3HMPA·toluene]: synthesis from reaction of solid NH 4 Br with Bu n Li in HMPA (hexamethylphosphoramide)/toluene media, crystal structure showing two Li–Br units linked by three µ 2 -HMPA ligands, and detection of 7 Li 31 P coupling in solutions of the complex
J. Chem. Soc., Chem. Commun.
(1989)
318
(doi: 10.1039/c39890000318)
A Li 8 cluster of three edge-connected Li 4 tetrahedra held by Li–N, Li C, and Li Li interactions: crystal structure of ( o -LiC 6 H 4 CH 2 ·NLi·CH 2 CH 2 NMe 2 ) 4 and detection of metal metal coupling within it by 7 Li COSY n.m.r. spectroscopy
Chemical Communications
(1988)
367
(doi: 10.1039/c39880000367)
Evidence for a radical-forming process during the reaction of solid NH 4 SCN with n-butyl-lithium and hexamethylphosphosphoramide (HMPA) in toluene: crystal structure of the product, (LiNCS·2HMPA) 2
Chemical Communications
(1988)
1415
(doi: 10.1039/c39880001415)
Synthesis and crystal and solution structures of the 1 : 1 TMEDA complex of lithium thiocyanate, (LiSCN·TMEDA)n[TMEDA = Me2N(CH2)2NMe2]: a polymeric solid with Li+ions linked by bifunctional linear SCN–ligands
J. Chem. Soc., Chem. Commun.
(1988)
145
(doi: 10.1039/c39880000145)
Isolation and solution structures of {PhCH2NLiCH2CH2NMe2}n and of the totally rigid dilithium compound, {o-LiC6H4CH2NLiCH2CH2NMe2}n; evidence for Li…o-HC interactions
Journal of Organometallic Chemistry
(1987)
325
c1
(doi: 10.1016/0022-328x(87)80411-4)
