Synthesis and crystal structure of Sb(N[double bond, length half m-dash]CPh 2 ) 3
J. Chem. Soc., Dalton Trans.
(1993)
2257
(doi: 10.1039/dt9930002257)
A model intermediate for the nucleophilic substitution of (Cp)2Sn; synthesis and structure of (Cp)(Me3Si)2NSn(µ-Cp)Li·pmdeta [Cp = C5H5, pmdeta =(Me2NCH2CH2)2NMe]
Chemical Communications
(1993)
1349
(doi: 10.1039/c39930001349)
The first calcium–mercury cocomplex: synthesis and crystal structure
J. Chem. Soc., Chem. Commun.
(1992)
573
(doi: 10.1039/c39920000573)
Isolation, structure and MO calculational investigations of a highly stable, hydrogen-bonded primary amine–phosphine oxide adduct, 2-aminobenzothiazole–HMPA, C6H4SC(N)NH2OP(NMe2)3; a possible model to explain the carcinogenicity of HMPA (HMPA = hexamethylphosphoramide)
Chemical Communications
(1992)
262
(doi: 10.1039/c39920000262)
The observation of a Pb–Li bond; synthesis, structure and model molecular orbital (MO) calculations on the monomeric Ph 3 Pb–Li·(pmdeta) complex [pmdeta =(Me 2 NCH 2 CH 2 ) 2 NMe]
Chemical Communications
(1992)
1413
(doi: 10.1039/c39920001413)
METAL-MEDIATED CONVERSION OF A 5-AMINOTHIATRIAZOLE INTO A 5-MERCAPTOTETRAZOLYL LIGAND BY REACTION WITH A SOLID METAL HYDROXIDE - SYNTHESIS AND CRYSTAL-STRUCTURE OF [CYCLO-NAPHTHYLN-BULLET-N=N-BULLET-N-RADICAL-ANIONC(RADICAL-ANIONS)]2BA-BULLET-3HMPA
J. Chem. Soc., Chem. Commun.
(1992)
1152
(doi: 10.1039/c39920001152)
THE STABILIZATION OF WATER AS A LIGAND IN LITHIATED ORGANIC-COMPOUNDS - INTRAMOLECULAR AND INTERMOLECULAR HYDROGEN-BONDING IN THE STRUCTURES OF THE AQUO COMPLEXES [C6H4OC(=S)=NLI-HMPA-H2O]2 AND [C6H4OC(=S)=NLI-HMPA]2-H2O
Inorganica Chimica Acta
(1991)
185
163
Lithiations of mercaptoamines containing NC(S)NH–,–NHC(S)S– and –NHC(S)NH– units: syntheses, crystal structures and model molecular-orbital calculations
Dalton Transactions
(1991)
765
(doi: 10.1039/dt9910000765)
The first lithiated organic compound containing water as a ligand: synthesis and crystal structure of 2-mercaptobenzoxazolyl(tetramethylethylenediamine)lithium monohydrate, C6H4OC(S)NLi(tmeda)H2O, a model acid–base intermediate
Chemical Communications
(1990)
643
(doi: 10.1039/c39900000643)
Unusual routes to complexes of binary alkali metal–non-metal compounds: preparations and crystal and solution structures of Li 2 S 6 ·(tmeda) 2 (tmeda = etramethylethylenediamine), and synthetic extensions of the routes
Chemical Communications
(1990)
105
(doi: 10.1039/c39900000105)
[H2C(CH2)5NLI]6, THE 1ST CYCLIZED LITHIUM AMIDE LADDER - SYNTHESIS AND STRUCTURE OF HEXAMETHYLENEIMIDOLITHIUM
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION IN ENGLISH
(1989)
28
1241
Dilithiation of N,N′-diphenylthiourea, PhNHC(S)NHPh, in HMPA: the unexpected structure of the product, [PhNLiC(NPh)SLi·2HMPA]2, and supporting ab initio MO calculations on model systems
Journal of Organometallic Chemistry
(1989)
362
C1
(doi: 10.1016/0022-328x(89)85298-2)
A unique lithium halide complex, [(LiBr)2·3HMPA·toluene]: synthesis from reaction of solid NH4Br with BunLi in HMPA (hexamethylphosphoramide)/toluene media, crystal structure showing two Li–Br units linked by three µ2-HMPA ligands, and detection of7Li ⋯31P coupling in solutions of the complex
Chemical Communications
(1989)
318
(doi: 10.1039/c39890000318)
Reaction of solid sodium hydride with solid ammonium thiocyanate in HMPA-toluene: An ESR spectroscopic investigation and crystal structures of the two products of the reaction, [(NaNCS·HMPA)2]∞ and (NaNCS·2HMPA)2
Polyhedron
(1989)
8
215
2 MONOMERIC, OCTAHEDRAL COMPLEXES OF ALKALINE-EARTH METAL-SALTS - SYNTHESES, PHYSICAL CHARACTERISTICS, AND CRYSTAL-STRUCTURES OF SRI2.4HMPA AND SR(NCS)2.4HMPA [HMPA=O-P(NME2)3]
J. Chem. Soc., Chem. Commun.
(1989)
893
(doi: 10.1039/c39890000893)
Evidence for a radical-forming process during the reaction of solid NH4SCN with n-butyl-lithium and hexamethylphosphosphoramide (HMPA) in toluene: crystal structure of the product, (LiNCS·2HMPA)2
J. Chem. Soc., Chem. Commun.
(1988)
1415
(doi: 10.1039/c39880001415)
A Li 8 cluster of three edge-connected Li 4 tetrahedra held by Li–N, Li C, and Li Li interactions: crystal structure of ( o -LiC 6 H 4 CH 2 ·NLi·CH 2 CH 2 NMe 2 ) 4 and detection of metal metal coupling within it by 7 Li COSY n.m.r. spectroscopy
J. Chem. Soc., Chem. Commun.
(1988)
367
(doi: 10.1039/c39880000367)
Synthesis and crystal and solution structures of the 1 : 1 TMEDA complex of lithium thiocyanate, (LiSCN·TMEDA) n [TMEDA = Me 2 N(CH 2 ) 2 NMe 2 ]: a polymeric solid with Li + ions linked by bifunctional linear SCN – ligands
J. Chem. Soc., Chem. Commun.
(1988)
145
(doi: 10.1039/c39880000145)
Isolation and solution structures of {PhCH2NLiCH2CH2NMe2}n and of the totally rigid dilithium compound, {o-LiC6H4CH2NLiCH2CH2NMe2}n; evidence for Li…o-HC interactions
Journal of Organometallic Chemistry
(1987)
325
c1
(doi: 10.1016/0022-328x(87)80411-4)
3 MODEL STRUCTURAL TYPES IN LITHIUM AMIDE CHEMISTRY - THE CRYSTAL AND MOLECULAR-STRUCTURES OF DIMERIC [PH(ME)NLI.ME2NCH2CH2NME2]2 AND MONOMERIC PH(NAPHTHYL)NLI.MEN(CH2CH2NME2)2 AND OF [PH(NAPHTHYL)NLI.TMEDA]2, A LOOSE DIMER
J. Chem. Soc., Chem. Commun.
(1987)
716
(doi: 10.1039/c39870000716)
