Senior Research Associate (X-Ray Crystallography)
Chemical Crystallography
Crystallographic methods provide detailed atomic-level descriptions of crystalline solids, including molecular structure and geometrical information on intermolecular interactions.
Single-crystal and powder X-ray diffraction are core analytical techniques within the chemical sciences, which support and augment a broad range of research within the Department. Modern diffraction instruments, applied at both laboratory and synchrotron sources, enable complex chemical problems to be tackled using crystallographic methods: for example, characterizing and understanding the consequences of disorder in molecular crystals or monitoring chemical changes in single crystals or crystalline powders.
Publications
Formation of Double Cubanes [Sn7(NR)8] in the Reactions of Pyridyl and Pyrimidinyl Amines with Sn(NMe2)2: A Synthetic and Theoretical Study †
– Inorg Chem
(2002)
41,
1492
(doi: 10.1021/ic011090r)
A 1:2 complex of pyromellitic diimide and dimethyl sulfoxide
– Acta Crystallographica Section E Structure Reports Online
(2002)
58,
o194
(doi: 10.1107/S1600536802001162)
Redetermination of the twinned structure of triacetone amine monohydrate.
– Acta crystallographica. Section C, Crystal structure communications
(2002)
58,
o115
(doi: 10.1107/s0108270101021527)
n-Decane
– Acta Crystallographica Section E: Crystallographic Communications
(2002)
58,
o196
(doi: 10.1107/S1600536802001332)
Synthesis, structures and coordination behaviour of [As(NR)3]3– trianions
– Journal of the Chemical Society Dalton Transactions
(2002)
343
(doi: 10.1039/b106913f)
Syntheses and structures of the cubanes [PhOSb(µ 3 -NCy)] 4 and [pyOBi(µ 3 -NCy)] 4 (Cy = cyclohexyl, py = 2-pyridyl)
– Dalton Transactions
(2002)
4629
(doi: 10.1039/B208302G)
Syntheses and magnetic properties of hexanuclear [Cp2Mn3(L1)4]2and octanuclear [Mn8(L2)12(μ4-O)2] (L1= 2-HNC5H5N, L2= 2-NH-3-Br-5-MeC5H3N, Cp = C5H5)
– Chemical Communications
(2002)
8,
2980
(doi: 10.1039/b209496g)
Design of luminescent polymers for leds
– Materials Research Society Symposium Proceedings
(2002)
708,
185
C-H⋯π interactions in the low-temperature crystal structures of α,Ω-unsaturated linear hydrocarbons
– Chemical Communications
(2002)
2,
1664
(doi: 10.1039/b204261d)
C–Hπ interactions in the low-temperature crystal structures of α,ω-unsaturated linear hydrocarbons
– Chem. Commun.
(2002)
1664
(doi: 10.1039/b204261d)
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