Senior Research Associate (X-Ray Crystallography)
Chemical Crystallography
Crystallographic methods provide detailed atomic-level descriptions of crystalline solids, including molecular structure and geometrical information on intermolecular interactions.
Single-crystal and powder X-ray diffraction are core analytical techniques within the chemical sciences, which support and augment a broad range of research within the Department. Modern diffraction instruments, applied at both laboratory and synchrotron sources, enable complex chemical problems to be tackled using crystallographic methods: for example, characterizing and understanding the consequences of disorder in molecular crystals or monitoring chemical changes in single crystals or crystalline powders.
Publications
Synthesis, structures and coordination behaviour of [As(NR)3]3- trianions
– Dalton Transactions
(2002)
343
(doi: 10.1039/b106913f)
Design of luminescent polymers for leds
– Materials Research Society Symposium - Proceedings
(2002)
708,
185
Syntheses and magnetic properties of hexanuclear [Cp2Mn3(L1)4]2 and octanuclear [Mn8(L2)12(mu 4-O)2] (L1 = 2-HNC5H5N, L2 = 2-NH-3-Br-5-MeC5H3N, Cp = C5H5).
– Chemical communications (Cambridge, England)
(2002)
8,
2980
(doi: 10.1039/b209496g)
Concomitant polymorphs: structural studies on the trimorphic dithiadiazolyl radical, ClCNSSN
– Journal of the Chemical Society, Dalton Transactions
(2002)
2522
(doi: 10.1039/b110922g)
Improved synthesis of dithieno[3,2-b:2′,3′-d] thiophene (DTT) and derivatives for cross coupling
– Chemical Communications
(2002)
2,
2424
(doi: 10.1039/b207403f)
C-H⋯π interactions in the low-temperature crystal structures of α,Ω-unsaturated linear hydrocarbons
– Chemical Communications
(2002)
2,
1664
(doi: 10.1039/b204261d)
C-H...pi interactions in the low-temperature crystal structures of alpha,omega-unsaturated linear hydrocarbons.
– Chem. Commun.
(2002)
1664
(doi: 10.1039/b204261d)
Syntheses and structures of the cubanes [PhOSb(mu(3)-NCy)](4) and [pyOBi(mu(3)-NCy)](4) (Cy = cyclohexyl, py=2-pyridyl)
– J. Chem. Soc., Dalton Trans.
(2002)
4629
(doi: 10.1039/B208302G)
Modification of the solid-state structure of bis(1-hydroxy-2(1 H )-pyridinethiolato- S 2 , O )zinc( ii ): synthesis and characterisation of a molecular solid solution incorporating 3-hydroxy-4-methyl-2(3 H )-thiazolethione
– Journal of Materials Chemistry
(2001)
12,
324
(doi: 10.1039/b106734f)
Molecular Conformation and Intermolecular Interactions in the Crystal Structures of Free-Base 5,15-Diarylporphyrins
– Crystal Growth and Design
(2001)
2,
27
(doi: 10.1021/cg010029u)
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