Senior Research Associate (X-Ray Crystallography)
Chemical Crystallography
Crystallographic methods provide detailed atomic-level descriptions of crystalline solids, including molecular structure and geometrical information on intermolecular interactions.
Single-crystal and powder X-ray diffraction are core analytical techniques within the chemical sciences, which support and augment a broad range of research within the Department. Modern diffraction instruments, applied at both laboratory and synchrotron sources, enable complex chemical problems to be tackled using crystallographic methods: for example, characterizing and understanding the consequences of disorder in molecular crystals or monitoring chemical changes in single crystals or crystalline powders.
Publications
Synthesis and characterization of a new layered compound of trimesic acidElectronic supplementary information (ESI) available: top view of the HxBTC anionic network (Fig. S1) and detailed hydrogen bond graph sets present in the interactions linking the two HxBTC sheets within a double layer (Fig. S2). See http://www.rsc.org/suppdata/nj/b1/b108083k/
New Journal of Chemistry
(2002)
26
381
(doi: 10.1039/b108083k)
Formation of double cubanes [SN7(NR)8] in the reactions of pyridyl and pyrimidinyl amines with Sn(NMe2)2: A synthetic and theoretical study
Inorg Chem
(2002)
41
1492
(doi: 10.1021/ic011090r)
Redetermination of the twinned structure of triacetone amine monohydrate
Acta Crystallographica Section C Crystal Structure Communications
(2002)
58
o115
(doi: 10.1107/s0108270101021527)
n-Decane
Acta Crystallographica Section E Structure Reports Online
(2002)
58
o196
(doi: 10.1107/s1600536802001332)
A 1:2 complex of pyromellitic diimide and dimethyl sulfoxide
Acta Crystallographica Section E Structure Reports Online
(2002)
58
o194
(doi: 10.1107/s1600536802001162)
Synthesis, structures and coordination behaviour of [As(NR)3]3- trianions
Journal of the Chemical Society, Dalton Transactions
(2002)
343
(doi: 10.1039/b106913f)
Syntheses and magnetic properties of hexanuclear [Cp2Mn3(L1)4]2 and octanuclear [Mn8(L2)12(μ4-O)2] (L1 = 2-HNC5H5N, L2 = 2-NH-3-Br-5-MeC5H3N, Cp = C5H5)
Chemical communications (Cambridge, England)
(2002)
8
2980
(doi: 10.1039/b209496g)
C-H⋯π interactions in the low-temperature crystal structures of α,Ω-unsaturated linear hydrocarbons
Chemical Communications
(2002)
2
1664
(doi: 10.1039/b204261d)
Concomitant polymorphs: structural studies on the trimorphic dithiadiazolyl radical, ClCNSSN
Journal of the Chemical Society, Dalton Transactions
(2002)
2522
(doi: 10.1039/b110922g)
Design of luminescent polymers for leds
Materials Research Society Symposium Proceedings
(2002)
708
185
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