Senior Research Associate (X-Ray Crystallography)
Chemical Crystallography
Crystallographic methods provide detailed atomic-level descriptions of crystalline solids, including molecular structure and geometrical information on intermolecular interactions.
Single-crystal and powder X-ray diffraction are core analytical techniques within the chemical sciences, which support and augment a broad range of research within the Department. Modern diffraction instruments, applied at both laboratory and synchrotron sources, enable complex chemical problems to be tackled using crystallographic methods: for example, characterizing and understanding the consequences of disorder in molecular crystals or monitoring chemical changes in single crystals or crystalline powders.
Publications
Nucleophilic addition to a Sn(II) imido cubane, [SnNR]4; a new route to heteroleptic stannates
– Journal of the Chemical Society, Dalton Transactions
(2002)
3525
(doi: 10.1039/b204340h)
2,3-lutidine
– Acta Crystallographica Section E Structure Reports Online
(2002)
58,
o961
(doi: 10.1107/S1600536802013648)
Templating and selection in the formation of macrocycles containing [{P(μ-NtBu)2}(μ-NH)]n frameworks: Observation of halide ion coordination
– Chemistry - A European Journal
(2002)
8,
3377
(Trimethylsilyl)acetylene
– Acta Crystallographica Section E Structure Reports Online
(2002)
58,
o777
(doi: 10.1107/S1600536802010875)
Synthesis and biological evaluation of phospholane and dihydrophosphole analogues of the glutamate receptor agonist AP4
– JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1
(2002)
2,
1625
(doi: 10.1039/b204891d)
Synthesis of a deca-lithium cage containing an [(RN)2As(mu-NR)As(NR)2]4- tetraanion; a homologue of group 15 trianions of the type [E(NR)3]3-.
– Chemical Communications
(2002)
2,
1276
(doi: 10.1039/b202858a)
Cobalt-mediated synthesis of angular [4]phenylene: Structural characterization of a metal lacyclopentadiene(alkyne) intermediate and its thermal and photochemical conversion
– Org Lett
(2002)
4,
2075
(doi: 10.1021/ol025956o)
Synthesis and X-ray crystal structures of bis(3-hydroxy-4-methyl-2(3H)-thiazolethiolato-S-2,O)bis(dimethylsulfoxide-O)M, M=cobalt(II) and nickel(II)
– Transition Metal Chemistry
(2002)
27,
407
(doi: 10.1023/A:1015067422886)
2,4-Lutidine
– Acta Crystallographica Section E: Crystallographic Communications
(2002)
58,
o550
(doi: 10.1107/s160053680200692x)
Supramolecular synthons in the co-crystal structures of 2-aminopyrimidine with diols and carboxylic acids
– Tetrahedron Letters
(2002)
43,
3101
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