Senior Research Associate (X-Ray Crystallography)
Chemical Crystallography
Crystallographic methods provide detailed atomic-level descriptions of crystalline solids, including molecular structure and geometrical information on intermolecular interactions.
Single-crystal and powder X-ray diffraction are core analytical techniques within the chemical sciences, which support and augment a broad range of research within the Department. Modern diffraction instruments, applied at both laboratory and synchrotron sources, enable complex chemical problems to be tackled using crystallographic methods: for example, characterizing and understanding the consequences of disorder in molecular crystals or monitoring chemical changes in single crystals or crystalline powders.
Publications
2,3-lutidine
Acta Crystallographica Section E: Crystallographic Communications
(2002)
58
o961
(doi: 10.1107/S1600536802013648)
Templating and selection in the formation of macrocycles containing [{P(μ-NtBu)2}(μ-NH)]n frameworks: Observation of halide ion coordination
Chemistry (Weinheim an der Bergstrasse, Germany)
(2002)
8
3377
(Trimethylsilyl)acetylene
Acta Crystallographica Section E Structure Reports Online
(2002)
58
O777
(doi: 10.1107/s1600536802010875)
Synthesis and biological evaluation of phospholane and dihydrophosphole analogues of the glutamate receptor agonist AP4Electronic supplementry information (ESI) available: mode of epoxide ring-opening and experimental data for 2 and 3. See http://www.rsc.org/suppdata/p1/b2/b204891d/
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1
(2002)
2
1625
(doi: 10.1039/b204891d)
Synthesis of a deca-lithium cage containing an [(RN) 2 As(μ-NR)As(NR) 2 ] 4− tetraanion; a homologue of group 15 trianions of the type [E(NR) 3 ] 3−
Chem Commun (Camb)
(2002)
2
1276
(doi: 10.1039/b202858a)
Cobalt-Mediated Synthesis of Angular [4]Phenylene: Structural Characterization of a Metallacyclopentadiene(Alkyne) Intermediate and Its Thermal and Photochemical Conversion
Organic Letters
(2002)
4
2075
(doi: 10.1021/ol025956o)
Synthesis and X-ray crystal structures of bis(3-hydroxy-4-methyl-2(3H)-thiazolethiolato-S2,O)bis(dimethylsulfoxide-O)M, M = cobalt(II) and nickel(II)
Transition Metal Chemistry
(2002)
27
407
(doi: 10.1023/a:1015067422886)
p-Phenylazophenacy Esters. Rates of Movement Relative to p-Phenylazophenacyl Bromide on Silicic Acid and Identification by Paper Partition Chromatography
Analytical Chemistry
(2002)
29
1162
(doi: 10.1021/ac60128a012)
2,4-Lutidine
Acta Crystallographica Section E: Crystallographic Communications
(2002)
58
o550
(doi: 10.1107/s160053680200692x)
Supramolecular synthons in the co-crystal structures of 2-aminopyrimidine with diols and carboxylic acids
Tetrahedron Letters
(2002)
43
3101
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