The NMR Service in B28 stock a wide range of deuterated solvents, shift reagents, and other ancilliary chemicals for use in NMR Spectroscopy We are your preferred supplier of the correct types of NMR tubes [Z274291-1PAK for 8 inch and Z272019-1PAK for 7 inch to use on SampleJet on Tobermory] to prepare your samples in, now priced at £8.50 per tube, plus NMR tube caps in various coloured packs of 100, priced at £9.30.
The following deuterated solvents are kept in stock, the prices are correct as of February 2021. Marketplace product prices from Merck (Sigma) are reviewed annually and the date of the rise will be noted on this website (2021 prices as listed below from 1st Feb 21 to 31st Jan 22). We have negotiated extremely favourable prices for the common items we buy in bulk from Fluorochem and Merck, and once our Merck vending machine is installed the prices will be lower still. Saving you and your PI's money and increasing the grant spend on actual NMR experiments!! Fill in the consumables request form available here.
| Solvent | Price per individual item (£) |
| Acetone ((CD3)2O) d6 0.75ml vial Sigma | 1.50 |
| Acetonitrile (CD3CN) d3 0.75ml vial Sigma | 1.60 |
| Benzene (C6D6) d6 0.75ml vial Sigma | 1.50 PRICE DROP |
| Dichloromethane (DCM CD2Cl2) d2 1ml vial Sigma | 2.80 |
| Methanol (CD3OD) d4 0.75ml vial Sigma | 1.40 |
| Pyridine (C6D5N) d5 0.75ml vial Fluorochem | 4.00 |
| Tetrahydrofuran (THF (CD2)4O) d8 0.75ml vial Fluorochem | 16.00 |
| Toluene (C7D8) d8 0.75ml vial Fluorochem | 7.10 |
| Acetone ((CD3)2O) d6 100% 0.75ml vial Fluorochem | 3.20 |
| Acetonitrile (CD3CN) d3 100% 0.75ml vial Fluorochem | 6.60 |
| Benzene (C6D6) d6 100% 0.75ml vial Fluorochem | 5.00 |
| Chloroform (CDCl3) d1 100% 0.75ml vial Sigma | 1.80 |
| Water (D2O) d2 100% 0.75ml vial Sigma | 1.50 |
| Dimethylsulfoxide (DMSO) d6 100% 0.75ml vial Sigma | 1.10 |
| Pyridine (C6D5N) d5 100% 0.75ml vial Fluorochem | 10.00 |
| Acetone ((CD3)2O) d6 10g Sigma - Glass screwtop bottle | 17.00 |
| Acetonitrile (CD3CN) d3 10ml Sigma - Glass screwtop bottle | 16.00 |
| Benzene (C6D6) d6 10g Sigma - Glass screwtop bottle | 27.50 |
| Dichloromethane (DCM CD2Cl2) d2 10g Sigma - Glass screwtop bottle | 28.00 |
| Dimethylsulfoxide (DMSO) d6 10g Sigma - Septa Seal bottle | 13.00 |
| Methanol d4 10g Sigma - Septa Seal bottle | 16.00 PRICE DROP |
| Tetrahydrofuran (THF (CD2)4O) d8 10g Sigma - Glass screwtop bottle | 75.00 PRICE DROP |
| Toluene (C7D8) d8 10g Sigma - Glass screwtop bottle | 35.00 PRICE DROP |
| Water (D2O) d2 100% 10g Sigma - Glass screwtop bottle | 15.00 |
| Chloroform (CDCl3) d1 100ml Fluorochem - Glass screwtop bottle | 20.00 |
| Chloroform (CDCl3) d1 100g Sigma - Glass screwtop bottle | 9.00 |
| Sodium Deuteroxide (NaOD) 30% wt soln. in D2O 20g Sigma | 47.00 |
| Deuterium Chloride (DCl) 10% wt soln. in D2O 10g Acros | 20.00 |
We have a range of other chemicals useful in NMR Spectroscopy. These include D2SO4, DCl (£19.00), Sodium 3 - Trimethylsilylpropionate-2,2,3,3 (TSP) (d4), 3-(Trimethylsilyl)-propansulphonic acid Na salt (DSS), Tetramethylsilane (TMS), and Sodium Deuteroxide. We also have some 'oddities' in our fridge which may be useful - please come and ask our advice.
